login
Updated 08/19/2026
11

Wafer cleaning issues at the wet process

Process description

The wet cleaning process is performed with single-wafer equipment, one by one.

The wafer rotates, and the chemistry or rinsing water is poured from the nozzle to the central area of the wafer, but it can also move from the center to the periphery of the wafer.

Equipment:

Failure and possible trigger:


  1. Defects were found on the wafer after the wet cleaning.
  2. The defects started appearing after the introduction of a new batch of chemistry (turn-on date):




  1. The comparative chemical analyses of the previous and suspected batches showed that all parameters for both batches are within specification limits.
  2. The only difference found is that the concentration of one of the components is slightly elevated in the suspected batch.
  3. Nevertheless, it is important to highlight that the elevated component remained well within the specification limits. See the chart below:





The traditional approach to problem-solving

The Problem

The new batch of chemistry is contaminated. The chemical content of the suspected batch does not match the typical composition of the chemistry.



Directions to solve this problem

  1. Remove the batch from the production line. Dispose or return it to the vendor and ask to prepare another batch with a purity that matches the typical batches.
  2. Change the specification limits to be tighter than the current to avoid similar excursions in the future.


The disadvantages of the traditional approach


  1. Cost increase – production cost will definitely be elevated
  2. Recurring excursions – similar excursions may occur again with the same or other components
  3. Lack of innovation – this solution is not improving the process or development of the technology


A systematic approach is needed. The usage of creative thinking tools is necessary for the generation of innovative ideas

Login to comment

Similar projects

This project applies Functional Modeling to analyze the single-wafer wet etch process in semiconductor manufacturing. The model shows that wet etch defects are not caused only by chemistry, but also by interactions between the wafer, liquid flow, air, rotation, rinsing, drying, drain, and chamber environment. Key challenges include incomplete wetting, trapped air or bubbles, residue and particle redeposition, evaporation-driven watermarks, and contamination during rinse or drying. The project identifies improvement directions such as better wafer pre-wetting, controlled airflow, reduced evaporation, optimized rinse and drying conditions, and alternative chamber concepts such as face-down processing in a shallow liquid bath.

Anatoly Agulyansky avatar
Anatoly Agulyansky
Alex Agulyansky avatar

The process is related to microelectronics - microchip manufacturing. The purpose of the process is to create a SiO2 layer on the surface of a Si wafer. Equipment: Vertical furnace to heat the wafers in the Q2 atmosphere and perform oxidation on the wafer surface. Process: The oxidation occurs on the front side and on the back side of the wafer Requirements: Create a SiO2 thin layer with a certain thickness and low sigma - low standard deviation of the thickness between the wafers and within the wafer Failure: Wafers from the lower zone have higher thickness and significantly higher within wafer sigma (standard deviation of the thickness within the wafer)

Anatoly Agulyansky avatar
Anatoly Agulyansky
Mike Agulyansky avatar
Anatoly Agulyansky avatar
Alex Agulyansky avatar

This project investigates particle-defect formation during SiO₂ dry etch. Functional modeling revealed that defects can be generated by two coupled mechanisms: chemical formation of SiO₂/SiOFₓ particles from SiF₄ interaction with moisture, and mechanical generation of particles by excessive ion bombardment and sputtering. The proposed improvement direction is to balance chemical etching and ion-assisted etching by properly adjusting the source and bias generators, reducing moisture, improving by-product evacuation, minimizing sputtering, and using pulsed or multi-step process recipes. The goal is to reduce particles and micromasking while maintaining etch rate, profile control, and process stability.

Anatoly Agulyansky avatar
Anatoly Agulyansky